ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Base Information

Chemical Name:ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate
CAS No.:124872-89-5
Molecular Formula:C₂₁H₂₂O₉
Molecular Weight:418.4
Hs Code.:

Synonyms:ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

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Chemical Property of ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

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Technology Process of ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

There total 3 articles about ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 57280-74-7
5-methoxy-2-(methoxymethoxy)phenol

: 81581-28-4
ethyl bromo-(3,4-methylenedioxybenzoyl)acetate

: 124872-89-5
ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: With potassium tert-butylate; dibenzo-18-crown-6; In acetonitrile; for 14h; Ambient temperature;

Reference yield:

: 73220-20-9
5-methoxy-2-(methoxymethoxy)benzaldehyde

: 124872-89-5
ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: m-chloroperbenzoic acid, KF / CH₂Cl₂ / Ambient temperature

2: aq. NaOH / 0.5 h / Ambient temperature

3: 90 percent / tert-BuOK / dibenzo-18-crown-6 / acetonitrile / 14 h / Ambient temperature

With potassium fluoride; potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; dibenzo-18-crown-6; In sodium hydroxide; dichloromethane; acetonitrile;

Reference yield:

: Formic acid 5-methoxy-2-methoxymethoxy-phenyl ester

: 124872-89-5
ethyl 2-<5'-methoxy-2'-(methoxymethoxy)phenoxy>-3-(3'',4''-methylenedioxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / 0.5 h / Ambient temperature

2: 90 percent / tert-BuOK / dibenzo-18-crown-6 / acetonitrile / 14 h / Ambient temperature

With potassium tert-butylate; dibenzo-18-crown-6; In sodium hydroxide; acetonitrile;