(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

Base Information

Chemical Name:(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide
CAS No.:108167-34-6
Molecular Formula:C₂₂H₂₀N₄O₆S
Molecular Weight:468.49
Hs Code.:

Synonyms:(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

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Chemical Property of (S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

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Technology Process of (S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

There total 5 articles about (S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 14193-18-1
3,5-dinitrobenzaldehyde

: 89556-73-0
(-)(S)-N-(α-methylbenzyl-N-benzylamine)sulfamide

: 108167-34-6
(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

Guidance literature:: With Amberlyst 15; 5A molecular sieve; In benzene; for 18h; Heating;
DOI:10.1021/ja00245a030

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 108167-34-6
(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / benzene / Heating

2: 90 percent / sodium borohydride

3: 78 percent / NH₂SO₂NH₂ / 1,2-dimethoxy-ethane / 144 h / Heating

4: 80 percent / 5 A molecular sieves, Amberlyst 15 / benzene / 18 h / Heating

With sodium tetrahydroborate; Amberlyst 15; 5A molecular sieve; SULFAMIDE; In 1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00245a030

Reference yield:

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 108167-34-6
(S)-N-(3,5-dinitrophenyl)-N'-(α-methylbenzyl)-N'-benzylsulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NH₂SO₂NH₂ / 1,2-dimethoxy-ethane / 144 h / Heating

2: 80 percent / 5 A molecular sieves, Amberlyst 15 / benzene / 18 h / Heating

With Amberlyst 15; 5A molecular sieve; SULFAMIDE; In 1,2-dimethoxyethane; benzene;
DOI:10.1021/ja00245a030