C₃₇H₅₆N₆O₈S₂

Base Information

Chemical Name:C₃₇H₅₆N₆O₈S₂
CAS No.:1443463-52-2
Molecular Formula:C₃₇H₅₆N₆O₈S₂
Molecular Weight:777.019
Hs Code.:

C<sub>37</sub>H<sub>56</sub>N<sub>6</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₃₇H₅₆N₆O₈S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₅₆N₆O₈S₂

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Technology Process of C₃₇H₅₆N₆O₈S₂

There total 12 articles about C₃₇H₅₆N₆O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1443463-50-0
C₃₇H₆₀N₆O₁₀S₂

: 1443463-52-2
C₃₇H₅₆N₆O₈S₂

Guidance literature:: With Burgess Reagent; In tetrahydrofuran; at 65 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201203667

Reference yield:

: 1443463-74-8
C₂₁H₂₆N₄O₄S

: 1443463-52-2
C₃₇H₅₆N₆O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; sodium nitrite / water / 0.5 h / 0 - 40 °C

2: tetrahydrofuran / 0 °C / Inert atmosphere

3: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4: Burgess Reagent / tetrahydrofuran / 1 h / 65 °C / Inert atmosphere

With Burgess Reagent; tetrabutyl ammonium fluoride; acetic acid; sodium nitrite; In tetrahydrofuran; water;
DOI:10.1002/chem.201203667

Reference yield:

: C₁₂H₂₄N₂O₄

: 1443463-52-2
C₃₇H₅₆N₆O₈S₂

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2: tetrahydrofuran / 0 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V) / dichloromethane / 0 - 20 °C / Inert atmosphere

4: tetrahydrofuran / 0 °C / Inert atmosphere

5: acetic acid; tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

6: Burgess Reagent / tetrahydrofuran / 1 h / 65 °C / Inert atmosphere

With Burgess Reagent; tetrabutyl ammonium fluoride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; acetic acid; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201203667