(1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate

Base Information

• Chemical Name: (1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate
• CAS No.: 1009368-80-2
• Molecular Formula: C₁₇H₂₂NO₄PS
• Molecular Weight: 367.406

Synonyms:(1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate

Chemical Property of (1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate

Chemical Property:

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Technology Process of (1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate

There total 1 articles about (1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

(1R,RP)-ethyl 1,1-diethoxyethyl(1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethyl)phosphinate → (1R,SP)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate (1009368-80-2)

Guidance literature:

With chloro-trimethyl-silane; ethanol; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tetasy.2007.11.021

Reference yield: 37.0%

Diazoethan (1117-96-0) + (1R,SP)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate (1009368-80-2) → (1R)-diethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphonate (1009368-74-4)

Guidance literature:

(1R,S_P)-ethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphinate; With iodine; dimethyl sulfoxide; In tetrahydrofuran; at 20 ℃; for 1h;

Diazoethan; In diethyl ether; ethanol; at 0 ℃; for 0.5h; Further stages.;

DOI:10.1016/j.tetasy.2007.11.021

Downstream raw materials:

(1R)-diethyl 1-{[(4-methylphenyl)sulfonyl]amino}-2-phenylethylphosphonate

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