C₅₅H₇₉IO₆S

Base Information

Chemical Name:C₅₅H₇₉IO₆S
CAS No.:1427381-93-8
Molecular Formula:C₅₅H₇₉IO₆S
Molecular Weight:995.199
Hs Code.:

C<sub>55</sub>H<sub>79</sub>IO<sub>6</sub>S

Synonyms:C₅₅H₇₉IO₆S

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Chemical Property of C₅₅H₇₉IO₆S

Chemical Property:

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Technology Process of C₅₅H₇₉IO₆S

There total 10 articles about C₅₅H₇₉IO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1427381-92-7
(2R,2'R,5S,5'S)-5,5'-bis((R)-1-(benzyloxy)-11-iodoundecyl)octahydro-2,2'-bifuran

: 184435-75-4
(5S)-5-methyl-3-phenylsulfanyl-4,5-dihydrofuran-2(3H)-one

: 1427381-93-8
C₅₅H₇₉IO₆S

Guidance literature:: With potassium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/j.tet.2013.02.015

Reference yield:

: 1427381-82-5
(4R,4'R,7R,7'R)-7,7'-bis((R,E)-1-(benzyloxy)-11-chloroundec-2-en-1-yl)-4,4',7,7'-tetrahydro-4,4'-bi(1,3-dioxepine)

: 1427381-93-8
C₅₅H₇₉IO₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; palladium 10% on activated carbon; hydrogen / 3 h / 20 °C / 760.05 Torr

2.1: hydrogenchloride / methanol / 5 h / Reflux

3.1: toluene-4-sulfonic acid / dichloromethane / 16 h / 20 °C

4.1: triethylamine / dichloromethane / 5 h / 20 °C

5.1: toluene-4-sulfonic acid / water; methanol / 5 h / 60 °C

5.2: 16 h / 20 °C

6.1: sodium iodide / acetone / 16 h / Reflux

7.1: potassium hydride / N,N-dimethyl-formamide / 16 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium hydride; toluene-4-sulfonic acid; triethylamine; sodium iodide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2013.02.015

Reference yield:

: 1427381-68-7
(3R,4R,8R,9R,13R,14R)-1,16-diphenyl-3,4,8,9,13,14-hexavinyl-2,5,7,10,12,15-hexaoxahexadecane

: 1427381-93-8
C₅₅H₇₉IO₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 3 h / 75 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 0.33 h / Inert atmosphere

2.2: Reflux; Inert atmosphere

3.1: triethylamine; palladium 10% on activated carbon; hydrogen / 3 h / 20 °C / 760.05 Torr

4.1: hydrogenchloride / methanol / 5 h / Reflux

5.1: toluene-4-sulfonic acid / dichloromethane / 16 h / 20 °C

6.1: triethylamine / dichloromethane / 5 h / 20 °C

7.1: toluene-4-sulfonic acid / water; methanol / 5 h / 60 °C

7.2: 16 h / 20 °C

8.1: sodium iodide / acetone / 16 h / Reflux

9.1: potassium hydride / N,N-dimethyl-formamide / 16 h / 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium hydride; toluene-4-sulfonic acid; triethylamine; sodium iodide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2013.02.015