C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆

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Chemical Name:C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆
CAS No.:82399-58-4
Molecular Formula:C₃₃H₃₅NOP₂Re*F₆P
Molecular Weight:854.766
Hs Code.:

C<sub>5</sub>H<sub>5</sub>Re(NO)CHP(CH<sub>3</sub>)3C<sub>6</sub>H<sub>5</sub>P(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=ReC<sub>5</sub>H<sub>5</sub>NOP(C<sub>6</sub>H<sub>5</sub>)3CHP(CH<sub>3</sub>)3C<sub>6</sub>H<sub>5</sub>PF<sub>6</sub>

Synonyms:C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆

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Chemical Property of C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆

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Technology Process of C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆

There total 1 articles about C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 74561-64-1
C₅H₅Re(NO)CHC₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=Re(C₅H₅)NOP(C₆H₅)3CHC₆H₅PF₆

: 594-09-2
trimethylphosphane

: 82399-58-4
C₅H₅Re(NO)CHP(CH₃)3C₆H₅P(C₆H₅)3⁽¹⁺⁾*PF₆^(1-)=ReC₅H₅NOP(C₆H₅)3CHP(CH₃)3C₆H₅PF₆

Guidance literature:: In dichloromethane; Re-complex was dissolved in CH2Cl2, cooled to -78°C, PMe3 was added, soln. was stirred for 5 min at -78°C under N2, mixt. was allowed to warm to room temp.; solvent was removed in vac., solid was taken up in CH2Cl2, hexane was layered onto soln., allowed to stand, filtered, dried;
DOI:10.1021/ja00382a021