2-(diethoxyphosphoryl)phenyloxymethylbenzene

Base Information

Chemical Name:2-(diethoxyphosphoryl)phenyloxymethylbenzene
CAS No.:252554-76-0
Molecular Formula:C₁₇H₂₁O₄P
Molecular Weight:320.325
Hs Code.:

Synonyms:2-(diethoxyphosphoryl)phenyloxymethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(diethoxyphosphoryl)phenyloxymethylbenzene

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Technology Process of 2-(diethoxyphosphoryl)phenyloxymethylbenzene

There total 1 articles about 2-(diethoxyphosphoryl)phenyloxymethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31575-75-4
2-bromophenyl benzyl ether

: 762-04-9
phosphonic acid diethyl ester

: 252554-76-0
2-(diethoxyphosphoryl)phenyloxymethylbenzene

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In dimethyl sulfoxide; at 100 ℃; for 12h;
DOI:10.1021/ja992493h

Reference yield: 17.0%

: 252554-76-0
2-(diethoxyphosphoryl)phenyloxymethylbenzene

: 252554-77-1
benzyl 2-(phosphino)phenyl ether

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 40 ℃; for 3h;
DOI:10.1021/jo062044h

Reference yield:

: 252554-76-0
2-(diethoxyphosphoryl)phenyloxymethylbenzene

: 2-[(2R,5R)-2,5-dimethylphospholano]phenyloxymethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 17 percent / LiAlH₄ / diethyl ether / 3 h / 40 °C

2: 58 percent / KH / tetrahydrofuran / 4 h / 20 °C

With lithium aluminium tetrahydride; potassium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo062044h