diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

Base Information

Chemical Name:diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate
CAS No.:101554-02-3
Molecular Formula:C₃₄H₃₇O₈P
Molecular Weight:604.637
Hs Code.:

Synonyms:diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

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Chemical Property of diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

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Technology Process of diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

There total 17 articles about diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 101554-02-3
diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: 49 percent / K₂CO₃-CuO / pyridine; quinoline / 170 °C

2: 84 percent / t-BuOk / dimethylformamide

3: H₂ / PtO₂

4: LiAlH₄

5: SOBr₂

With lithium aluminium tetrahydride; sulfurous dibromide; potassium tert-butylate; hydrogen; potassium carbonate; copper(II) oxide; platinum(IV) oxide; In pyridine; quinoline; N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587

Reference yield:

: 3132-99-8
m-bromobenzoic aldehyde

: 101554-02-3
diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: 49 percent / K₂CO₃-CuO / pyridine; quinoline / 170 °C

2: 84 percent / t-BuOk / dimethylformamide

3: H₂ / PtO₂

4: LiAlH₄

5: SOBr₂

With lithium aluminium tetrahydride; sulfurous dibromide; potassium tert-butylate; hydrogen; potassium carbonate; copper(II) oxide; platinum(IV) oxide; In pyridine; quinoline; N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587

Reference yield:

: 621-59-0
isovanillin

: 101554-02-3
diethyl <3-methoxy-4-<3-<2-<4-(2-methoxy-5-formylphenoxy)phenyl>ethyl>phenoxy>benzyl>phosphonate

Guidance literature:: Multi-step reaction with 11 steps

1: 79 percent / K₂CO₃-CuO / pyridine / Heating

2: p-TsOH

3: LiAlH₄

4: SOBr₂

6: p-TsOH

7: 84 percent / t-BuOk / dimethylformamide

8: H₂ / PtO₂

9: LiAlH₄

10: SOBr₂

With lithium aluminium tetrahydride; sulfurous dibromide; potassium tert-butylate; hydrogen; potassium carbonate; copper(II) oxide; platinum(IV) oxide; toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587