trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

Base Information

Chemical Name:trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine
CAS No.:847830-46-0
Molecular Formula:C₄₈H₄₈N₁₀
Molecular Weight:764.976
Hs Code.:

trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1<i>H</i>-tetrazol-5-yl]-ethyl}-amine

Synonyms:trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

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Chemical Property of trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

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Technology Process of trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

There total 2 articles about trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 847830-42-6
3-(trityl-amino)-N-{4-[3-(trityl-amino)-thiopropionylamino]-butyl}-thiopropionamide

: 847830-46-0
trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

Guidance literature:: With trimethylsilylazide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 25 ℃; for 24h;
DOI:10.1021/ol0477069

Reference yield:

: 168699-00-1
3-(Trityl-amino)-N-{4-[3-(trityl-amino)-propionylamino]-butyl}-propionamide

: 847830-46-0
trityl-{2-[1-(4-{5-[2-(trityl-amino)-ethyl]-tetrazol-1-yl}-butyl)-1H-tetrazol-5-yl]-ethyl}-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Lawesson's reagent / tetrahydrofuran / 2 h / Heating

2: 55 percent / trimethylsilyl azide; triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 24 h / 25 °C

With Lawessons reagent; trimethylsilylazide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/ol0477069