(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

Base Information

Chemical Name:(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester
CAS No.:113453-58-0
Molecular Formula:C₂₈H₃₈O₅
Molecular Weight:454.607
Hs Code.:

Synonyms:(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

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Technology Process of (2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

There total 5 articles about (2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96481-55-9,2088-07-5
2-methylpent-1-en-3-ol

: 113453-58-0
(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1) (+)-diisopropyl tartrate, Ti(O-i-Pr)4; 2) TBHP / 1) CH₂Cl₂, -20 deg C, 15 min; 2) benzene, -20 deg C, 33 h

2: 90 percent / NaH / tetrahydrofuran; dimethylformamide / 4 h / 0 °C

3: 100 percent / tetrahydrofuran / 16 h / Ambient temperature

4: 95 percent / KH / tetrahydrofuran / 25 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; potassium hydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja00216a026

Reference yield:

: 84599-41-7
(R^*,S^*)-α-Ethyl-2-methyloxiranemethanol

: 113453-58-0
(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaH / tetrahydrofuran; dimethylformamide / 4 h / 0 °C

2: 100 percent / tetrahydrofuran / 16 h / Ambient temperature

3: 95 percent / KH / tetrahydrofuran / 25 °C

With potassium hydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja00216a026

Reference yield:

: 113474-72-9
<2R,2(1S)>-2-<1-<(4-methoxyphenyl)methoxy>propyl>-2-methyloxirane

: 113453-58-0
(2E,6R,7S)-7-<(4-methoxyphenyl)methoxy>-2,6-dimethyl-6-(phenylmethoxy)-2-nonenoic acid, ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / tetrahydrofuran / 16 h / Ambient temperature

2: 95 percent / KH / tetrahydrofuran / 25 °C

With potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00216a026