O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Base Information

Chemical Name:O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate
CAS No.:1541178-53-3
Molecular Formula:C₃₇H₃₆F₃NO₇
Molecular Weight:663.691
Hs Code.:

Synonyms:O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Chemical Property:

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Technology Process of O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

There total 3 articles about O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 127873-80-7,127873-97-6,127874-23-1,127875-22-3,127875-29-0,127875-36-9
3-O-acetyl-2,4,6-tri-O-benzyl-D-glycopyranose

: 1541178-53-3
O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

: 1541179-64-9
O-(3-O-acetyl-2,4,6-tri-O-benzyl-β-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; Overall yield = 94 %; Overall yield = 132 mg;
DOI:10.1016/j.carres.2013.11.016

Reference yield:

: 89104-66-5
1,3-di-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranose

: 1541178-53-3
O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

: 1541179-64-9
O-(3-O-acetyl-2,4,6-tri-O-benzyl-β-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazinium monoacetate / N,N-dimethyl-formamide / 1.5 h / 20 °C

2: potassium carbonate / acetone

With hydrazinium monoacetate; potassium carbonate; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.carres.2013.11.016

Reference yield:

: 35303-86-7
(2R,3S,4S,5R,6S)-3,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-4-ol

: 1541178-53-3
O-(3-O-acetyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl) N-phenyltrifluoroacetimidate

: 1541179-64-9
O-(3-O-acetyl-2,4,6-tri-O-benzyl-β-D-glucopyranosyl) N-phenyltrifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; acetic anhydride / water / 1 h / Reflux

2: hydrazinium monoacetate / N,N-dimethyl-formamide / 1.5 h / 20 °C

3: potassium carbonate / acetone

With hydrogenchloride; hydrazinium monoacetate; acetic anhydride; potassium carbonate; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.carres.2013.11.016