ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

Base Information

Chemical Name:ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate
CAS No.:232603-06-4
Molecular Formula:C₃₂H₃₈O₇
Molecular Weight:534.65
Hs Code.:

Synonyms:ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

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Chemical Property of ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

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Technology Process of ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

There total 4 articles about ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-oct-6-enopyranoside)uronate

: 232603-06-4
ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethyl acetate; at 20 ℃; for 12h; under 1810.07 Torr;
DOI:10.1021/jo0005159

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 232603-06-4
ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: Swern reagent / CH₂Cl₂; dimethylsulfoxide / 0.5 h / -78 °C

2: 85 percent / benzene / 4 h / 20 °C

3: 95 percent / H₂ / Lindlar catalyst / ethyl acetate / 12 h / 20 °C / 1810.07 Torr

With swern reagent; hydrogen; Lindlar's catalyst; In dichloromethane; dimethyl sulfoxide; ethyl acetate; benzene; 1: Swern oxidation / 2: Wittig reaction / 3: Catalytic hydrogenation;
DOI:10.1021/jo0005159

Reference yield:

: 83051-88-1
methyl 6-aldehydo-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 232603-06-4
ethyl (methyl 2,3,4-tri-O-benzyl-6,7-dideoxy-α-D-gluco-octopyranosid)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / benzene / 4 h / 20 °C

2: 95 percent / H₂ / Lindlar catalyst / ethyl acetate / 12 h / 20 °C / 1810.07 Torr

With hydrogen; Lindlar's catalyst; In ethyl acetate; benzene; 1: Wittig reaction / 2: Catalytic hydrogenation;
DOI:10.1021/jo0005159