5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

Base Information

Chemical Name:5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole
CAS No.:1380244-77-8
Molecular Formula:C₅₂H₅₄N₂S
Molecular Weight:739.08
Hs Code.:

Synonyms:5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

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Chemical Property of 5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

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Technology Process of 5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

There total 5 articles about 5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1380244-76-7
2,2'-(dibenzo[b,d]thiophene-3,7-diyl)bis(N-(4-octylphenyl)aniline)

: 1380244-77-8
5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

Guidance literature:: With copper diacetate; palladium diacetate; In toluene; at 80 ℃; for 48h; Inert atmosphere;

Reference yield:

: 16245-79-7
4-octylaniline

: 1380244-77-8
5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium t-butanolate / palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 100 °C / Inert atmosphere

2: triethylamine / DavePhos; palladium diacetate / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere

3: potassium phosphate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 48 h / 90 °C / Inert atmosphere

4: copper diacetate / palladium diacetate / toluene / 48 h / 80 °C / Inert atmosphere

With potassium phosphate; copper diacetate; triethylamine; sodium t-butanolate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; DavePhos; In 1,4-dioxane; water; toluene;

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 1380244-77-8
5,8-bis(4-octylphenyl)-5,8-dihydrothieno[3,2-b:4,5-b']dicarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: sodium t-butanolate / palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 24 h / 100 °C / Inert atmosphere

2: triethylamine / DavePhos; palladium diacetate / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere

3: potassium phosphate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane; water / 48 h / 90 °C / Inert atmosphere

4: copper diacetate / palladium diacetate / toluene / 48 h / 80 °C / Inert atmosphere

With potassium phosphate; copper diacetate; triethylamine; sodium t-butanolate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; DavePhos; In 1,4-dioxane; water; toluene;