2-Hydroxylamino-4-nitroanisole

Base Information

• Chemical Name: 2-Hydroxylamino-4-nitroanisole
• CAS No.: 13027-36-6
• Molecular Formula: C₇H₈N₂O₄
• Molecular Weight: 184.152
• DSSTox Substance ID: DTXSID901284769

Synonyms:2-hydroxylamino-4-nitroanisole;DTXSID901284769;N-Hydroxy-2-methoxy-5-nitrobenzenamine;13027-36-6

Chemical Property of 2-Hydroxylamino-4-nitroanisole

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 184.04840674
• Heavy Atom Count: 13
• Complexity: 182

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)[N+](=O)[O-])NO

Technology Process of 2-Hydroxylamino-4-nitroanisole

There total 3 articles about 2-Hydroxylamino-4-nitroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

2,4-dinitroanisole (119-27-7) + triethylamine (121-44-8) → N-hydroxy-2-methoxy-5-nitroaniline (13027-36-6) + 4-methoxy-3-nitroaniline (577-72-0) + N-ethyl-4-nitro-2-nitrosoaniline + N-ethyl-2-hydroxylamino-4-nitroaniline + 3-amino-4-methoxynitrobenzene (99-59-2)

Guidance literature:

With benzophenone; In isopropyl alcohol; for 3h; Product distribution; Irradiation;

DOI:10.1016/S0040-4020(01)89963-4

Reference yield:

2,4-dinitroanisole (119-27-7) → N-hydroxy-2-methoxy-5-nitroaniline (13027-36-6) + 2,2'-dimethoxy-5,5'-dinitroazoxybenzene (13027-37-7)

Guidance literature:

bei der elektrolytischen Reduktion an einer Silberkathode;

Reference yield:

→ N-hydroxy-2-methoxy-5-nitroaniline (13027-36-6)

Guidance literature:

2,4-Dinitro-anisol/ NH4Ac+A. bei 20grad (elektrol. Red.);

upstream raw materials:

2,4-dinitroanisole

triethylamine

Downstream raw materials:

2,2'-dimethoxy-5,5'-dinitroazoxybenzene

3-amino-4-methoxynitrobenzene

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