(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

Base Information

Chemical Name:(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate
CAS No.:1164114-97-9
Molecular Formula:C₅₆H₉₆O₁₁Si₃
Molecular Weight:1029.63
Hs Code.:

(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

Synonyms:(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

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Chemical Property of (2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

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Technology Process of (2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

There total 1 articles about (2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1164115-15-4
C₅₂H₉₀O₁₀Si₃

: 16139-79-0
ethyl diphenylphosphonoacetate

: 1164114-97-9
(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

Guidance literature:: ethyl diphenylphosphonoacetate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

C₅₂H₉₀O₁₀Si₃; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - -20 ℃; Inert atmosphere;
DOI:10.1021/ol900757k

Reference yield: 93.0%

: 1164114-97-9
(2Z,4S,5S,6E)-ethyl-7-((4R,5R)-4-(2-(tert-butyldimethylsilyloxy)ethyl)-2-(2,4-dimethoxyphenyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)-4-ethyl-5-(triethylsilyloxy)hepta-2,6-dienoate

: 1164115-16-5
C₄₄H₆₈O₁₁Si

Guidance literature:: With triethylamine tris(hydrogen fluoride); In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol900757k