Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)

Base Information

Chemical Name:Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)
CAS No.:763102-78-9
Molecular Formula:C₉H₁₈N₂O₄
Molecular Weight:218.253
Hs Code.:
Mol file:763102-78-9.mol

Synonyms:Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)

Suppliers and Price of Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI)

There total 5 articles about Butanoic acid, 3-amino-4-[[(1,1-dimethylethoxy)carbonyl]amino]-, (3R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108919-51-3
L-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyric acid

: 763102-78-9
(R)-3-Amino-4-tert-butoxycarbonylamino-butyric acid

Guidance literature:: With hydrogen; palladium; In methanol; water;
DOI:10.1021/jm00391a030

Reference yield:

: 16947-84-5,62234-36-0
N-[(benzyloxy)carbonyl]-3-[(tert-butoxycarbonyl)amino]-L-alanine

: 763102-78-9
(R)-3-Amino-4-tert-butoxycarbonylamino-butyric acid

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethylmorpholine / ethyl acetate / 1 h / 0 °C

2: diethyl ether / 13 h / 0 - 20 °C

3: silver benzoate, triethylamine / 4 h / Ambient temperature

4: 85 percent / 1 N aq. NaOH / methanol / 3 h / Ambient temperature

5: H₂ / Pd-black / methanol; H₂O

With N-ethylmorpholine;; sodium hydroxide; hydrogen; silver benzoate; triethylamine; palladium; In methanol; diethyl ether; water; ethyl acetate;
DOI:10.1021/jm00391a030

Reference yield:

: 108919-50-2
methyl L-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

: 763102-78-9
(R)-3-Amino-4-tert-butoxycarbonylamino-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 1 N aq. NaOH / methanol / 3 h / Ambient temperature

2: H₂ / Pd-black / methanol; H₂O

With sodium hydroxide; hydrogen; palladium; In methanol; water;
DOI:10.1021/jm00391a030