N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

Base Information

Chemical Name:N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride
CAS No.:1258945-83-3
Molecular Formula:C₂₃H₃₄N₂S₂*ClH
Molecular Weight:439.129
Hs Code.:

Synonyms:N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

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Technology Process of N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

There total 4 articles about N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1258945-80-0
N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine

: 1258945-83-3
N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

Guidance literature:: With nickel(II) chloride hexahydrate; In ethanol; for 12h; Reflux;
DOI:10.1007/s11172-010-0121-4

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 1258945-83-3
N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / water / 1.67 h / 0 °C

2: triethylamine / dichloromethane / 0 °C / Inert atmosphere

3: borane-THF / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

4: nickel(II) chloride hexahydrate / ethanol / 12 h / Reflux

With borane-THF; nickel(II) chloride hexahydrate; sulfuric acid; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1007/s11172-010-0121-4

Reference yield:

: 1258945-79-7
N,N'-bis[2-(tert-butylthio)phenyl]malonamide

: 1258945-83-3
N,N'-bis[2-(tert-butylthio)phenyl]propane-1,3-diamine monohydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

2: nickel(II) chloride hexahydrate / ethanol / 12 h / Reflux

With borane-THF; nickel(II) chloride hexahydrate; In tetrahydrofuran; ethanol;
DOI:10.1007/s11172-010-0121-4