5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine

Base Information

• Chemical Name: 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine
• CAS No.: 148144-68-7
• Molecular Formula: C₄₇H₄₄N₄O₁₂
• Molecular Weight: 856.886

Synonyms:5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine

Chemical Property of 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine

Chemical Property:

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Technology Process of 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine

There total 3 articles about 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O⁴-<2-(4-nitrophenyl)ethyl>thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride (88091-70-7) + 5'-O-(monomethoxytrityl)-O4-<2-(4-nitrophenyl)ethyl>thymidine (87875-16-9) → 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O4-<2-(4-nitrophenyl)ethyl>thymidine (148144-68-7)

Guidance literature:

With dmap; In dichloromethane;

DOI:10.1002/hlca.19930760122

Reference yield:

O4-<2-(4-nitrophenyl)ethyl>thymidine (87875-15-8) → 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O4-<2-(4-nitrophenyl)ethyl>thymidine (148144-68-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / pyridine / 28 h / Ambient temperature

2: 89 percent / 4-dimethylaminopyridine / CH₂Cl₂

With pyridine; dmap; In dichloromethane;

DOI:10.1002/hlca.19930760122

Reference yield:

mono-4-methoxytrityl chloride (14470-28-1) → 5'-O-(monomethoxytrityl)-3'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-O4-<2-(4-nitrophenyl)ethyl>thymidine (148144-68-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / pyridine / 28 h / Ambient temperature

2: 89 percent / 4-dimethylaminopyridine / CH₂Cl₂

With pyridine; dmap; In dichloromethane;

DOI:10.1002/hlca.19930760122

upstream raw materials:

1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride

5'-O-(monomethoxytrityl)-O⁴-<2-(4-nitrophenyl)ethyl>thymidine

O⁴-<2-(4-nitrophenyl)ethyl>thymidine

mono-4-methoxytrityl chloride

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