potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

Base Information

Chemical Name:potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate
CAS No.:85414-81-9
Molecular Formula:C₁₉H₁₉N₂O₇S₂*K
Molecular Weight:490.599
Hs Code.:

Synonyms:potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

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Chemical Property of potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

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Technology Process of potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

There total 7 articles about potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 85414-81-9
potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.8 g / propan-2-ol / 8 h / Heating

2: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; hydrogen; palladium on activated charcoal; In isopropyl alcohol;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 85414-81-9
potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 50 percent / butan-2-one / 6 h / Heating

3: 3.5 g / K₃CO₃ / N,N-dimethyl-acetamide / 1 h / 70 °C

4: 1.8 g / propan-2-ol / 8 h / Heating

5: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; ammonia; hydrogen; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl acetamide; isopropyl alcohol; butanone;
DOI:10.1021/jm00362a017

Reference yield:

: 100-67-4
potassium phenolate

: 85414-81-9
potassium N-furfuryl-4-phenoxy-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / butan-2-one / 6 h / Heating

2: 3.5 g / K₃CO₃ / N,N-dimethyl-acetamide / 1 h / 70 °C

3: 1.8 g / propan-2-ol / 8 h / Heating

4: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl acetamide; isopropyl alcohol; butanone;
DOI:10.1021/jm00362a017