Technology Process of C23H24N4O3
There total 7 articles about C23H24N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H30N4O3;
With
trifluoroacetic acid;
at 20 ℃;
for 1.5h;
With
sodium hydrogencarbonate; ammonium chloride;
In
water;
pH=6;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: ammonia / water / 12 h / 20 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / pyridine / 2 h / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 18 h / 20 °C
4.1: ethanol / 0.5 h / 140 °C / Microwave irradiation
5.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 0 - 20 °C
6.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
7.1: trifluoroacetic acid / 1.5 h / 20 °C
7.2: pH 6
With
hydrogenchloride; ammonia; potassium carbonate; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
pyridine; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethanol / 0.5 h / 140 °C / Microwave irradiation
2.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 0 - 20 °C
3.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
4.1: trifluoroacetic acid / 1.5 h / 20 °C
4.2: pH 6
With
hydrogenchloride; caesium carbonate; trifluoroacetic acid;
In
ethanol; ethyl acetate; N,N-dimethyl-formamide;
