1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

Base Information

Chemical Name:1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole
CAS No.:1446281-86-2
Molecular Formula:C₂₄H₃₁N₃
Molecular Weight:361.53
Hs Code.:

Synonyms:1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

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Chemical Property of 1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

Chemical Property:

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Technology Process of 1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

There total 6 articles about 1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50365-34-9
2-(piperidin-1-ylmethyl)-1H-benzo[d]imidazole

: 1446281-94-2
2-(3-bromopropyl)-1,3-dimethylbenzene

: 1446281-86-2
1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;

Reference yield:

: 608-28-6
2,6-dimethyliodobenzene

: 1446281-86-2
1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; diisopropylamine / tetrahydrofuran / 50 °C / Inert atmosphere; Reflux

2: hydrogen; platinum(IV) oxide / ethanol / 2534.09 - 3102.97 Torr

3: triphenylphosphine; carbon tetrabromide / dichloromethane / 3.17 h / 20 °C / Cooling with ice

4: potassium carbonate / N,N-dimethyl-formamide / 100 °C

With platinum(IV) oxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; carbon tetrabromide; hydrogen; potassium carbonate; diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 110-89-4
piperidine

: 1446281-86-2
1-[3-(2,6-dimethylphenyl)propyl]-2-piperidin-1-ylmethyl-1H-benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 1.75 h / -5 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 100 °C

With potassium carbonate; In N,N-dimethyl-formamide;