(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

Base Information

Chemical Name:(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate
CAS No.:851009-55-7
Molecular Formula:C₂₂H₃₃O₆P
Molecular Weight:424.474
Hs Code.:

Synonyms:(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

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Technology Process of (6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

There total 3 articles about (6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 851009-33-1
(5E,7E)-10-(4-methoxybenzyloxy)-7-methyldeca-5,7-dienoic acid methyl ester

: 756-79-6
dimethyl methane phosphonate

: 851009-55-7
(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h;
DOI:10.1021/ol050191g

Reference yield:

: (E)-(6-methoxy-6-oxohex-1-en-1-yl)boronic acid

: 851009-55-7
(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / Tl₂CO₃ / Pd(PPh₃)4 / tetrahydrofuran; H₂O / 0.5 h / 23 °C

2: 95 percent / n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 °C

With n-butyllithium; Ti₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; water; 1: Suzuki coupling reaction;
DOI:10.1021/ol050191g

Reference yield:

: 500702-36-3
(2E)-2-iodo-5-[(4-methoxybenzyl)oxy]pent-2-ene

: 851009-55-7
(6E,8E)-11-(4-methoxybenzyloxy)-8-methyl-2-oxoundeca-6,8-dienyldimethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / Tl₂CO₃ / Pd(PPh₃)4 / tetrahydrofuran; H₂O / 0.5 h / 23 °C

2: 95 percent / n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 °C

With n-butyllithium; Ti₂CO₃; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; water; 1: Suzuki coupling reaction;
DOI:10.1021/ol050191g