1-benzyloxy-18-phenyloctadecane

Base Information

Chemical Name:1-benzyloxy-18-phenyloctadecane
CAS No.:144878-57-9
Molecular Formula:C₃₁H₄₈O
Molecular Weight:436.722
Hs Code.:

Synonyms:1-benzyloxy-18-phenyloctadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyloxy-18-phenyloctadecane

Chemical Property:

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Technology Process of 1-benzyloxy-18-phenyloctadecane

There total 9 articles about 1-benzyloxy-18-phenyloctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 144878-52-4
17-benzyloxy-1-bromoheptadecane

: 144878-50-2
24-octadecyl-23-dotetraconten-19-one

: 144878-57-9
1-benzyloxy-18-phenyloctadecane

: 19-benzyl-24-octadecyl-23-dotetraconten-19-ol

: 144878-54-6
19-(17'-hydroxyheptadecyl)-24-octadecyl-23-dotetraconten-19-ol

: 144878-53-5
19-(17'-benzyloxyheptadecyl)-24-octadecyl-23-dotetraconten-19-ol

Guidance literature:: With lithium-sodium alloy; In tetrahydrofuran; hexane; at 50 ℃; for 1.5h; Further byproducts given; sonication;

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 144878-57-9
1-benzyloxy-18-phenyloctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / 55percent NaH in oil, BuNI / tetrahydrofuran / 2 h, rt. then reflux, 2 h

2: 44 percent / 1.) Mg, 1,2-dibromoethane; 2.) CuCl₂, LiCl / tetrahydrofuran / 1.) reflux, 2 h; 2.) -15 deg C, 6 h

3: 0.2 g / Li, Na / hexane / 1.5 h / 50 °C / ultrasonic bath

With sodium; tetra-(n-butyl)ammonium iodide; lithium; sodium hydride; magnesium; ethylene dibromide; lithium chloride; copper dichloride; In tetrahydrofuran; hexane;
DOI:10.1055/s-1993-25968

Reference yield:

: 144878-51-3
11-bromoundecan-1-yl benzyl ether

: 144878-57-9
1-benzyloxy-18-phenyloctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / 1.) Mg, 1,2-dibromoethane; 2.) CuCl₂, LiCl / tetrahydrofuran / 1.) reflux, 2 h; 2.) -15 deg C, 6 h

2: 0.2 g / Li, Na / hexane / 1.5 h / 50 °C / ultrasonic bath

With sodium; lithium; magnesium; ethylene dibromide; lithium chloride; copper dichloride; In tetrahydrofuran; hexane;
DOI:10.1055/s-1993-25968