5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

Base Information

Chemical Name:5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane
CAS No.:114719-11-8
Molecular Formula:C₂₇H₄₀N₂O₅
Molecular Weight:472.625
Hs Code.:

Synonyms:5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

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Chemical Property of 5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

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Technology Process of 5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

There total 9 articles about 5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 36839-55-1
1,2-bis-(2-iodoethoxy)ethane

: 114719-14-1
6-(hydroxymethyl)-1,12-diphenyl-2,11-diaza-5,8-dioxadodecane

: 114719-11-8
5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

Guidance literature:: With sodium carbonate; sodium iodide; In acetonitrile; for 25h; Heating;
DOI:10.1021/jo00249a012

Reference yield: 15.0%

: 114719-09-4
5-<(allyloxy)methyl>-1,10-dibenzyl-2,9-dioxo-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

: 114719-11-8
5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

: 114719-03-8
5-<(allyloxy)methyl>-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 36h; Heating;
DOI:10.1021/jo00249a012

Reference yield:

: 107106-47-8
(1,4,10,13-tetraoxa-7,16-diazacyclooctadecan-2-yl)methanol

: 100-44-7
benzyl chloride

: 114719-11-8
5-hydroxymethyl-1,10-dibenzyl-4,7,13,16-tetraoxa-1,10-diazacyclooctadecane

Guidance literature:: (1,4,10,13-tetraoxa-7,16-diazacyclooctadecan-2-yl)methanol; With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 0.25h;

benzyl chloride; In tetrahydrofuran;