2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

Base Information

Chemical Name:2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid
CAS No.:58632-19-2
Molecular Formula:C₁₆H₁₇N₃O₆
Molecular Weight:347.327
Hs Code.:

2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2<i>H</i>-pyrimidin-1-yl)-propionic acid

Synonyms:2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

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Chemical Property of 2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

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Technology Process of 2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

There total 2 articles about 2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 26054-60-4
((S)-2-Oxo-oxetan-3-yl)-carbamic acid benzyl ester

: 65-71-4,28806-14-6,691841-57-3
thymin

: 58632-19-2
2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1039/b822789f

Reference yield:

: 58632-19-2
2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

Guidance literature:: Carbobenzoxychlorid, β-(1-Thyminyl)-α-alanin;
DOI:10.1007/BF00474466

Reference yield: 40.0%

: 4512-32-7
H-Aib-OtBu

: 58632-19-2
2-benzyloxycarbonylamino-3-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-propionic acid

: C₂₄H₃₂N₄O₇

Guidance literature:: With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 120h; pH=8.5;
DOI:10.1039/b822789f