Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester

Base Information

Chemical Name:Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester
CAS No.:879553-77-2
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:
ChEMBL ID:CHEMBL161029
DSSTox Substance ID:DTXSID601219406

Synonyms:CHEMBL161029;SCHEMBL7378851;Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester;DTXSID601219406;BDBM50085123;879553-77-2;2-(2-Benzyloxycarbonylamino-3-methyl-butyrylamino)-3-methyl-butyric acid (0.25H2O)

Suppliers and Price of Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:350.18417193
Heavy Atom Count:25
Complexity:458

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)C(C(=O)NC(C(C)C)C(=O)O)NC(=O)OCC1=CC=CC=C1

Technology Process of Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester

There total 2 articles about Valine, N-(N-carboxy-DL-valyl)-, DL-, N-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 879553-76-1
N-(N-benzyloxycarbonyl-valyl)-valine ethyl ester

: 879553-77-2
optically inactive N-(N-benzyloxycarbonyl-valyl)-valine

Guidance literature:: With sodium hydroxide;

Reference yield:

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 879553-77-2
optically inactive N-(N-benzyloxycarbonyl-valyl)-valine

Guidance literature:: Multi-step reaction with 2 steps

1: chlorocarbonic acid benzyl ester; aqueous NaOH

2: tributylamine; chlorocarbonic acid ethyl ester; dioxane / anschliessend Behandeln mit DL-Valin und wss. NaOH

With 1,4-dioxane; sodium hydroxide; tributyl-amine; chloroformic acid ethyl ester; benzyl chloroformate;