1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

Base Information

Chemical Name:1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline
CAS No.:1350322-17-6
Molecular Formula:C₂₀H₁₅N₇O₂
Molecular Weight:385.385
Hs Code.:

Synonyms:1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

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Chemical Property of 1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

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Technology Process of 1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

There total 2 articles about 1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1350322-12-1
2-[N'-((3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)methylidene)hydrazino]-3-methylquinoxaline

: 1350322-17-6
1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

Guidance literature:: 2-[N'-((3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)methylidene)hydrazino]-3-methylquinoxaline; With copper dichloride; In N,N-dimethyl-formamide; at 50 - 100 ℃; for 1.33333h; Inert atmosphere;

With ammonia; sodium chloride; In water; N,N-dimethyl-formamide; at 40 ℃; for 0.333333h; Air atmosphere;
DOI:10.1016/j.ejmech.2011.10.032

Reference yield:

: 51144-19-5
(3-methyl-quinoxalin-2-yl)-hydrazine

: 73225-31-7
C₁₁H₉N₃O₃

: 1350322-17-6
1-(3-methyl-1-(p-nitrophenyl)-1H-pyrazol-4-yl)-4-methyl-1,2,4-triazolo[4,3-a]quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / ethanol / 1 h / Reflux

2.1: copper dichloride / N,N-dimethyl-formamide / 1.33 h / 50 - 100 °C / Inert atmosphere

2.2: 0.33 h / 40 °C / Air atmosphere

With acetic acid; copper dichloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.10.032