5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

Base Information

Chemical Name:5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde
CAS No.:1352009-93-8
Molecular Formula:C₁₄H₁₃NO₃
Molecular Weight:243.262
Hs Code.:

Synonyms:5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

Suppliers and Price of 5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

Chemical Property:

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Technology Process of 5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

There total 2 articles about 5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1352009-71-2
5-(dimethylamino)-2,2-dimethyl-3-oxo-N-phenylpent-4-enamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1352009-93-8
5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trifluoromethylsulfonic anhydride; Cooling with ice;

5-(dimethylamino)-2,2-dimethyl-3-oxo-N-phenylpent-4-enamide; at 100 ℃; for 0.5h;
DOI:10.1021/ol203124f

Reference yield:

: 28252-07-5
2,2-dimethyl-3-oxo -N-phenylbutanamide

: 1352009-93-8
5,5-dimethyl-4,6-dioxo-1-phenyl-1,4,5,6-tetrahydropyridine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 5.08 h / 20 - 85 °C / Reflux

2.1: trifluoromethylsulfonic anhydride / Cooling with ice

2.2: 0.5 h / 100 °C

With trifluoromethylsulfonic anhydride; In N,N-dimethyl-formamide; 2.1: Vilsmeier type reaction / 2.2: Vilsmeier type reaction;
DOI:10.1021/ol203124f