1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

Base Information

Chemical Name:1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile
CAS No.:871116-98-2
Molecular Formula:C₁₅H₁₆N₄O
Molecular Weight:268.318
Hs Code.:

Synonyms:1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

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Chemical Property of 1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

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Technology Process of 1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

There total 1 articles about 1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 871116-97-1
3-(1-cyano-cyclobutyl)-5-[1,2,4]triazol-1-ylmethyl-benzoic acid methyl ester

: 871116-98-2
1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

Guidance literature:: With sodium tetrahydroborate; polyethylene glycol 400; at 80 ℃;
DOI:10.1039/b707768h

Reference yield: 92.0%

: 871116-98-2
1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

: 62262-84-4
methanesulfonic acid 4-mercaptophenyl ester

: methanesulfonic acid 4-[3-(1-cyanocyclobutyl)-5-[1,2,4]triazol-1-ylmethylbenzylsulfanyl]phenyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; propiononitrile; (cyanomethyl)trimethyl-phosphonium iodide; at 92 ℃;
DOI:10.1039/b707768h

Reference yield: 30.0%

: 871116-98-2
1-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)cyclobutanecarbonitrile

: 66952-59-8
methanesulfonic acid 2-chloro-4-mercaptophenyl ester

: 4({3-[(1H-1,2,4-triazol-1-yl)methyl]-5-(1-cyanocyclobutyl)benzyl}sulfanyl)-2-chlorophenyl methanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; propiononitrile; (cyanomethyl)trimethyl-phosphonium iodide; at 92 ℃;
DOI:10.1039/b707768h