4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane

Base Information

• Chemical Name: 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane
• CAS No.: 566168-49-8
• Molecular Formula: C₄₀H₆₂N₄O₆
• Molecular Weight: 694.955
• Mol file: 566168-49-8.mol

Synonyms:4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane

Chemical Property of 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane

There total 3 articles about 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-nitro-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane (566168-45-4) → 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane (566168-49-8)

Guidance literature:

With hydrogen; nickel; In ethanol; at 60 ℃; for 48h;

DOI:10.1016/S0040-4020(03)00463-0

Reference yield:

tris(2-cyanoethyl)nitromethane (1466-48-4) → 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane (566168-49-8)

Guidance literature:

Multi-step reaction with 3 steps

1: BH₃*THF / tetrahydrofuran / 4 h / Heating

2: 25 percent / methanol; CH₂Cl₂

3: 75 percent / H₂ / Raney nickel / ethanol / 48 h / 60 °C

With borane-THF; hydrogen; nickel; In tetrahydrofuran; methanol; ethanol; dichloromethane;

DOI:10.1016/S0040-4020(03)00463-0

Reference yield:

4-(3-aminopropyl)-4-nitroheptane-1,7-diamine (155021-55-9) → 4-amino-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane (566168-49-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 25 percent / methanol; CH₂Cl₂

2: 75 percent / H₂ / Raney nickel / ethanol / 48 h / 60 °C

With hydrogen; nickel; In methanol; ethanol; dichloromethane;

DOI:10.1016/S0040-4020(03)00463-0

upstream raw materials:

4-nitro-1,7-bis{N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}-4-{3-N-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl]amino}propylheptane

tris(2-cyanoethyl)nitromethane

4-(3-aminopropyl)-4-nitroheptane-1,7-diamine