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Technology Process of (3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

(3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

Base Information
  • Chemical Name:(3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline
  • CAS No.:1242105-69-6
  • Molecular Formula:C18H21NO
  • Molecular Weight:267.371
  • Hs Code.:
(3R,4R)-N<sup>(2)</sup>,3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

Synonyms:(3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of (3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline
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Technology Process of (3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about (3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(1R,2R)-1-phenyl-2-[N-methyl-N-(3'-methoxybenzyl)amino]propan-1-ol
1242105-58-3

(1R,2R)-1-phenyl-2-[N-methyl-N-(3'-methoxybenzyl)amino]propan-1-ol

(3R,4R)-N<sup>(2)</sup>,3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline
1242105-69-6

(3R,4R)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

(3R,4S)-N<sup>(2)</sup>,3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline
1242105-66-3

(3R,4S)-N(2),3-dimethyl-4-phenyl-7-methoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:
With sulfuric acid; trifluoroacetic acid; In dichloromethane; at 40 ℃; for 1.75h; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/asia.200900470
upstream raw materials:

(1R,2R)-1-phenyl-2-[N-methyl-N-(3'-methoxybenzyl)amino]propan-1-ol

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