O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

Base Information

Chemical Name:O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate
CAS No.:1597422-16-6
Molecular Formula:C₂₉H₃₀Cl₃NO₅
Molecular Weight:578.92
Hs Code.:

Synonyms:O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

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Chemical Property of O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

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Technology Process of O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

There total 1 articles about O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 545-06-2
trichloroacetonitrile

: 2,3,4-tri-O-benzyl-6-deoxy-D-galactopyranose

: 1597422-16-6
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

: O-(2,3,4-tri-O-benzyl-6-deoxy-β-D-galactopyranosyl) trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c4ob00241e

Reference yield: 93.0%

: 1597422-16-6
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

: C₂₆H₄₀O₇S

: C₅₃H₆₈O₁₁S

Guidance literature:: With C₂₉H₁₉F₄O₄P; In toluene; at 20 ℃; for 48h; Concentration; Time; Solvent; regioselective reaction; Molecular sieve;
DOI:10.1021/jacs.7b03198

Reference yield: 69.0%

: 1597422-16-6
O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate

: 1597422-19-9
(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-3-benzyloxy-2-hexacosanoylamidooctadec-4-ene

: 1597422-21-3
(2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-3-O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl)-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-3-benzyloxy-2-hexacosanoylamidooctadec-4-ene

Guidance literature:: O-(2,3,4-tri-O-benzyl-6-deoxy-α-D-galactopyranosyl) trichloroacetimidate; (2S,3R,4E)-1-(4-O-(4-O-acetyl-2,6-di-O-benzoyl-β-D-galactopyranosyl)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyloxy)-3-benzyloxy-2-hexacosanoylamidooctadec-4-ene; In dichloromethane; for 3h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃; for 21h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c4ob00241e