benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester

Base Information

• Chemical Name: benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester
• CAS No.: 1041171-73-6
• Molecular Formula: C₂₃H₂₆O₆
• Molecular Weight: 398.456
• Mol file: 1041171-73-6.mol

Synonyms:benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester

Chemical Property of benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester

There total 1 articles about benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C23H28O6 (1041171-58-7) → benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester (1041171-73-6)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

DOI:10.1021/ol801292t

Reference yield: 80.0%

benzoic acid (1S,3R)-3-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-1-methyl-2-oxobutyl ester (1041171-73-6) → (R)-2-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-pentan-3-one (1041171-60-1)

Guidance literature:

With methanol; samarium diiodide; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/ol801292t

upstream raw materials:

C₂₃H₂₈O₆

Downstream raw materials:

(R)-2-[(R)-2-(4-methoxy-phenyl)-[1,3]dioxan-4-yl]-pentan-3-one