(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

Base Information

Chemical Name:(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol
CAS No.:914803-06-8
Molecular Formula:C₃₇H₆₂O₁₀Si
Molecular Weight:694.979
Hs Code.:

Synonyms:(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

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Chemical Property of (3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

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Technology Process of (3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

There total 3 articles about (3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₅₈O₁₀Si

: 914803-06-8
(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 25 ℃; for 1h;
DOI:10.1002/ejoc.200600276

Reference yield:

: 914803-04-6
(2R,4S)-1,5-Bis-((2R,4S)-4-benzyloxymethoxy-6-hydroxy-tetrahydro-pyran-2-yl)-pentane-2,4-diol

: 914803-06-8
(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / CH₂Cl₂ / 1.5 h / -50 °C

2: 99 mg / NaBH₄ / methanol / 1 h / 25 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1002/ejoc.200600276

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 914803-06-8
(3R,5R,7S,9S,11S,13R)-3,13-Bis-benzyloxymethoxy-9-(tert-butyl-dimethyl-silanyloxy)-pentadecane-1,5,7,11,15-pentaol

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / CH₂Cl₂ / 1.5 h / -50 °C

2: 99 mg / NaBH₄ / methanol / 1 h / 25 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; In methanol; dichloromethane;
DOI:10.1002/ejoc.200600276