N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide
CAS No.:1218785-93-3
Molecular Formula:C₂₂H₂₅NO₂S
Molecular Weight:367.512
Hs Code.:

Synonyms:N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10285-80-0
N-tosyl-3-butenylamine

: 59163-81-4
2-methylene-1-phenylbut-3-en-1-ol

: 61201-27-2
1-phenylpenta-4,5-dien-1-ol

: 1218786-15-2
C₂₂H₂₅NO₂S

: 1218785-93-3
N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja100409b

Reference yield: 70.0%

: 1218785-93-3
N-(but-3-enyl)-N-(2-methylene-1-phenylbut-3-enyl)-4-methylbenzenesulfonamide

: 3-methyl-2-phenyl-1-tosyl-3,4-divinylpyrrolidine

Guidance literature:: With silver hexafluoroantimonate; tris(triphenylphosphine)rhodium(l) chloride; In 1,2-dichloro-ethane; at 65 ℃; for 2h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja100409b