C₃₅H₆₄O₅Si₂

Base Information

Chemical Name:C₃₅H₆₄O₅Si₂
CAS No.:944052-12-4
Molecular Formula:C₃₅H₆₄O₅Si₂
Molecular Weight:621.061
Hs Code.:

C<sub>35</sub>H<sub>64</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₅H₆₄O₅Si₂

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Chemical Property of C₃₅H₆₄O₅Si₂

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Technology Process of C₃₅H₆₄O₅Si₂

There total 13 articles about C₃₅H₆₄O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944052-05-5
C₂₈H₄₂O₄Si

: 944052-12-4
C₃₅H₆₄O₅Si₂

Guidance literature:: Multi-step reaction with 11 steps

1: 70 percent / Et₃N; DMAP / CH₂Cl₂ / 0 - 20 °C

2: 92 percent / TBAF / tetrahydrofuran / 0 - 20 °C

3: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 - 0 °C

4: CH₂Cl₂ / 20 °C

5: 86 percent / LiBH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

6: 96 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 0 - 20 °C

7: 65 percent / TFA / 2-methyl-propan-2-ol / 2 h / 20 °C

8: 100 percent / 2,6-lutidine / 0.17 h / 0 °C

9: 75 percent / HF; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

10: SO₃; pyridine; DMSO / CH₂Cl₂ / 0.5 h / 0 - 20 °C

11: CH₂Cl₂ / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; lithium borohydride; oxalyl dichloride; hydrogen fluoride; sulfur trioxide; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.04.016

Reference yield:

: C₃₂H₄₄O₄Si

: 944052-12-4
C₃₅H₆₄O₅Si₂

Guidance literature:: Multi-step reaction with 13 steps

1: 98 percent / CSA / CH₂Cl₂ / 0 - 20 °C

2: 78 percent / Li; liq. NH₃ / tetrahydrofuran / 0.17 h / -33 °C

3: 70 percent / Et₃N; DMAP / CH₂Cl₂ / 0 - 20 °C

4: 92 percent / TBAF / tetrahydrofuran / 0 - 20 °C

5: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 - 0 °C

6: CH₂Cl₂ / 20 °C

7: 86 percent / LiBH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

8: 96 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 0 - 20 °C

9: 65 percent / TFA / 2-methyl-propan-2-ol / 2 h / 20 °C

10: 100 percent / 2,6-lutidine / 0.17 h / 0 °C

11: 75 percent / HF; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

12: SO₃; pyridine; DMSO / CH₂Cl₂ / 0.5 h / 0 - 20 °C

13: CH₂Cl₂ / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; lithium borohydride; oxalyl dichloride; camphor-10-sulfonic acid; hydrogen fluoride; sulfur trioxide; tetrabutyl ammonium fluoride; ammonia; sodium hexamethyldisilazane; lithium; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.04.016

Reference yield:

: 944052-04-4
C₃₅H₄₈O₄Si

: 944052-12-4
C₃₅H₆₄O₅Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: 78 percent / Li; liq. NH₃ / tetrahydrofuran / 0.17 h / -33 °C

2: 70 percent / Et₃N; DMAP / CH₂Cl₂ / 0 - 20 °C

3: 92 percent / TBAF / tetrahydrofuran / 0 - 20 °C

4: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 - 0 °C

5: CH₂Cl₂ / 20 °C

6: 86 percent / LiBH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

7: 96 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 0 - 20 °C

8: 65 percent / TFA / 2-methyl-propan-2-ol / 2 h / 20 °C

9: 100 percent / 2,6-lutidine / 0.17 h / 0 °C

10: 75 percent / HF; pyridine / tetrahydrofuran / 5 h / 0 - 20 °C

11: SO₃; pyridine; DMSO / CH₂Cl₂ / 0.5 h / 0 - 20 °C

12: CH₂Cl₂ / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; lithium borohydride; oxalyl dichloride; hydrogen fluoride; sulfur trioxide; tetrabutyl ammonium fluoride; ammonia; sodium hexamethyldisilazane; lithium; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2007.04.016