[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

Base Information

Chemical Name:[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF
CAS No.:1158589-82-2
Molecular Formula:C₄H₈O*C₃₉H₆₀Cl₂N₃O₃Sc
Molecular Weight:806.893
Hs Code.:

[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl<sub>2</sub>(THF)3]*THF

Synonyms:[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

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Technology Process of [(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

There total 1 articles about [(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 928797-95-9
1,3-bis(2,6-diisopropylphenyl)-1H-imidazol-2(3H)-imine

: 10361-84-9
scandium(III) chloride

: 1158589-82-2
[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

Guidance literature:: With trimethylsilylmethyl lithium; In tetrahydrofuran; mixt. of ScCl3 and LiCH2SiMe3 treated with THF; stirred for 2 h; soln. of ligand in THF added; stirred for 12 h; solvent evapd.; repeatedly extd. with pentane; recrystd. from THF-pentane at -30°C; elem. anal.;
DOI:10.1021/ic900503q

Reference yield: 72.0%

: 1158589-82-2
[(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)ScCl₂(THF)3]*THF

: 34480-05-2
dipotassium cyclooctatetraenide

: [(η8-cycloctatetraenide)Sc(1,3-bis(2,6-diisopropylphenyl)imidazolin-2-iminato)(THF)]*THF

Guidance literature:: In tetrahydrofuran; soln. of Sc complex in THF treated with freshly prepared K2C8H8; stirredfor 12 h; solvent evapd.; extd. with pentane; filtered; evapd.; recrystd. from THF-pentane at -30°C; elem. anal.;
DOI:10.1021/ic900503q