(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

Base Information

Chemical Name:(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate
CAS No.:1071476-60-2
Molecular Formula:C₃₄H₃₇F₃N₄O₉S
Molecular Weight:734.75
Hs Code.:

Synonyms:(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

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Chemical Property of (S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

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Technology Process of (S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

There total 5 articles about (S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1071476-59-9
(S)-methyl 2-((S)-2-azido-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1071476-60-2
(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

Guidance literature:: With dmap; In acetonitrile; at 23 ℃;

Reference yield:

: 1071477-16-1
C₂₂H₂₅F₃N₂O₅*ClH

: 1071476-60-2
(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; sodium azide; trifluoromethylsulfonic anhydride; copper(II) sulfate / water / 0 - 23 °C

2: triethylamine / dichloromethane / 0.33 h / 0 °C

3: dmap / acetonitrile / 23 °C

With pyridine; dmap; sodium azide; trifluoromethylsulfonic anhydride; copper(II) sulfate; triethylamine; In dichloromethane; water; acetonitrile;

Reference yield:

: 1071476-58-8
(S)-methyl 2-((S)-2-azido-3-(4-(2-hydroxyethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

: 1071476-60-2
(S)-methyl 2-((S)-2-azido-N-(tert-butoxycarbonyl)-3-(4-(2-(tosyloxy)ethoxy)phenyl)propanamido)-3-(4-(trifluoromethyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.33 h / 0 °C

2: dmap / acetonitrile / 23 °C

With dmap; triethylamine; In dichloromethane; acetonitrile;