(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

Base Information

Chemical Name:(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal
CAS No.:93170-61-7
Molecular Formula:C₂₉H₂₈O₈S₃
Molecular Weight:600.735
Hs Code.:

Synonyms:(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

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Technology Process of (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

There total 1 articles about (2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 72263-10-6
2L-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone

: 540-63-6
ethane-1,2-dithiol

: 93170-61-7
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/0008-6215(84)85276-3

Reference yield: 97.0%

: 93170-61-7
(2S)-(2,4,5/3)-2,3-dibenzoyloxy-5-hydroxy-4-toluene-p-sulphonyloxycyclohexanone ethylene dithioacetal

: 93170-65-1
6-benzoyloxy-2,3-dihydro-1,4-benzodithiin

Guidance literature:: With N-Bromosuccinimide; N,N-dimethyl-formamide; triphenylphosphine; In 1,2-dimethoxyethane; at 105 ℃; for 32h;
DOI:10.1016/0008-6215(84)85276-3