1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Base Information

Chemical Name:1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal
CAS No.:99249-39-5
Molecular Formula:C₂₆H₃₂O₄
Molecular Weight:408.538
Hs Code.:

Synonyms:1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Chemical Property of 1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Technology Process of 1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

There total 1 articles about 1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 932-66-1
1-cyclohexenyl methyl ketone

: 99249-39-5
1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: pyridinium p-toluenesulfonate; In benzene; Heating;
DOI:10.1016/S0040-4020(01)90002-X

Reference yield:

: 75-11-6
diiodomethane

: 99249-39-5
1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 99249-40-8
(4S,5S)-4,5-Bis-benzyloxymethyl-2-(1R,6R)-bicyclo[4.1.0]hept-1-yl-2-methyl-[1,3]dioxolane

: 99295-92-8
(4S,5S)-4,5-Bis-benzyloxymethyl-2-(1S,6S)-bicyclo[4.1.0]hept-1-yl-2-methyl-[1,3]dioxolane

Guidance literature:: With zinc copper; iodine; In diethyl ether; Yield given. Yields of byproduct given; Heating;
DOI:10.1021/ja00312a073

Reference yield:

: 99249-39-5
1-cyclohexen-1-yl methyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: (1R,6R)-1-Bicyclo[4.1.0]hept-1-yl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: zinc-copper couple, iodine / diethyl ether / Heating

2: 86 percent / 3percent aq. sulfuric acid / tetrahydrofuran / 3.5 h / Ambient temperature

With zinc copper; sulfuric acid; iodine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00312a073