3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

Base Information

Chemical Name:3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol
CAS No.:1198109-61-3
Molecular Formula:C₂₀H₂₂ClN₅O
Molecular Weight:383.881
Hs Code.:

Synonyms:3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

Chemical Property:

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Technology Process of 3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

There total 4 articles about 3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198109-60-2
3-chloro-4-(6-chloro-2,8-dimethyl-purin-9-yl)-phenol

: 13375-29-6
dicyclopropylmethylamine

: 1198109-61-3
3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

Guidance literature:: In acetonitrile; at 160 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 2-chloro p-aminophenol hydrochloride

: 1198109-61-3
3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 2-methoxy-ethanol; water / 1 h / 160 °C / Microwave irradiation

1.2: pH 7

2.1: toluene-4-sulfonic acid / ethanol / 16 h / 80 °C / Inert atmosphere

3.1: acetonitrile / 0.5 h / 160 °C / Microwave irradiation

With hydrogenchloride; toluene-4-sulfonic acid; In ethanol; 2-methoxy-ethanol; water; acetonitrile;

Reference yield:

: 39906-04-2
5-amino-4,6-dichloro-2-methylpyrimidine

: 1198109-61-3
3-chloro-4-[6-(dicyclopropylmethylamino)-2,8-dimethyl-purin-9-yl]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 2-methoxy-ethanol; water / 1 h / 160 °C / Microwave irradiation

1.2: pH 7

2.1: toluene-4-sulfonic acid / ethanol / 16 h / 80 °C / Inert atmosphere

3.1: acetonitrile / 0.5 h / 160 °C / Microwave irradiation

With hydrogenchloride; toluene-4-sulfonic acid; In ethanol; 2-methoxy-ethanol; water; acetonitrile;