N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

Base Information

Chemical Name:N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one
CAS No.:138384-50-6
Molecular Formula:C₂₄H₁₈N₂O₃S
Molecular Weight:414.485
Hs Code.:

N<sup>6</sup>-<4-(phenylsulfonyl)benzyl>-6-aminobenz<cd>indol-2(1H)-one

Synonyms:N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

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Chemical Property of N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

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Technology Process of N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

There total 7 articles about N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50964-11-9
6-aminobenzindol-2(1H)-one

: 7705-63-7
1-(bromomethyl)-4-(phenylsulfonyl)benzene

: 138384-50-6
N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 75 ℃; for 3h;
DOI:10.1021/jm00082a006

Reference yield:

: 130-00-7
1,8-naphtholactam

: 138384-50-6
N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / 70percent HNO₃ / acetic acid / 1 h / 20 - 50 °C

2: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

3: 71 percent / DIEA / dimethylformamide / 3 h / 75 °C

With hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a006

Reference yield:

: 28434-96-0
N-hydroxy-4-nitro-1,8-naphthalimide

: 138384-50-6
N⁶-<4-(phenylsulfonyl)benzyl>-6-aminobenzindol-2(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂CO₃ / H₂O / 1 h / Heating

2: NaOH / ethanol; H₂O / 16 h / 25 °C

3: H₂ / 5percent Pd/C / tetrahydrofuran / 16 h / 2068.6 Torr

4: 71 percent / DIEA / dimethylformamide / 3 h / 75 °C

With sodium hydroxide; hydrogen; sodium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00082a006