3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride

Base Information

• Chemical Name: 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride
• CAS No.: 85197-53-1
• Molecular Formula: C₃₇H₄₅NO₅S*ClH
• Molecular Weight: 652.295
• Mol file: 85197-53-1.mol

Synonyms:3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride

Chemical Property of 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride

There total 2 articles about 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β,21-diacetoxypregna-5,16-dien-20-one (37413-93-7) → 3β,21-diacetoxy-16α,17α-epiminopregn-5-ene-3β,21-diol-20-one (83109-30-2) + 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride (85197-53-1)

Guidance literature:

With S,S-diphenylsulfylimine; In dichloromethane; at 20 ℃; for 24h; under 4560000 Torr;

DOI:10.1007/BF00950664

Reference yield:

S,S-Diphenylsulfilimine (36744-90-8) + 3β,21-diacetoxypregna-5,16-dien-20-one (37413-93-7) → 3β,21-diacetoxy-16α,17α-epiminopregn-5-ene-3β,21-diol-20-one (83109-30-2) + 3β,21-diacetoxy-16α-S,S-diphenylsulfyliminopregn-5-en-20-one hydrochloride (85197-53-1)

Guidance literature:

With dichloromethane; at 20 ℃; for 24h; under 4560000 Torr; Product distribution; Mechanism; further ketosteroids;

DOI:10.1007/BF00950664

upstream raw materials:

S,S-Diphenylsulfilimine

3β,21-diacetoxypregna-5,16-dien-20-one