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Technology Process of diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

Base Information
  • Chemical Name:diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate
  • CAS No.:1215019-55-8
  • Molecular Formula:C46H62N7O6P
  • Molecular Weight:840.015
  • Hs Code.:
diisopropyl (3R,4R)-3-{[N<sub>6</sub>-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

Synonyms:diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

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Chemical Property of diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate
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Technology Process of diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

There total 1 articles about diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C<sub>25</sub>H<sub>44</sub>N<sub>7</sub>O<sub>4</sub>P
1215019-56-9

C25H44N7O4P

4,4'-dimethoxytrityl chloride
40615-36-9

4,4'-dimethoxytrityl chloride

diisopropyl (3R,4R)-3-{[N<sub>6</sub>-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate
1215019-55-8

diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

Guidance literature:
With pyridine; silver trifluoromethanesulfonate; at 20 ℃;
DOI:10.1135/cccc2009022

Reference yield: 68.0%

diisopropyl (3R,4R)-3-{[N<sub>6</sub>-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate
1215019-55-8

diisopropyl (3R,4R)-3-{[N6-(dibutylamino)methyleneadenin-9-yl]-4-(4,4'-dimethoxytrityl)oxypyrrolidin-1-yl}methylphosphonate

C<sub>40</sub>H<sub>50</sub>N<sub>7</sub>O<sub>6</sub>P
1215019-58-1

C40H50N7O6P

Guidance literature:
With trimethylsilyl bromide; lutidine; In acetonitrile; at 20 ℃; Inert atmosphere; Enzymatic reaction;
DOI:10.1135/cccc2009022
upstream raw materials:

C25H44N7O4P

4,4'-dimethoxytrityl chloride

Downstream raw materials:

C40H50N7O6P

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