IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

Base Information

Chemical Name:IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄
CAS No.:132959-02-5
Molecular Formula:BF₄*C₅₅H₄₄IrO₅OsP₄
Molecular Weight:1378.07
Hs Code.:

IrOs(CO)5((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup> = {IrOs(CO)5(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)2}BF<sub>4</sub>

Synonyms:IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

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Chemical Property of IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

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Technology Process of IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

There total 1 articles about IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 132939-86-7
IrOs(H)2(CO)3((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(H)2(CO)3(((C₆H₅)2P)2CH₂)2}BF₄

: 132959-02-5
IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

Guidance literature:: With CO; In dichloromethane; (Ar); stirred a soln. of Ir-complex under a stream of CO for 36 h; evapd. (vac.); washed with THF and Et2O; recrystd. from CH2Cl2/Et2O; elem. anal.;
DOI:10.1021/om00051a018

Reference yield: 70.0%

: 132959-02-5
IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

: 132939-90-3
IrOs(CO)4((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)4(((C₆H₅)2P)2CH₂)2}BF₄

Guidance literature:: With (CH₃)3NO*2H₂O; In acetonitrile; (Ar); added dropwise a soln. of (CH3)3NO*2H2O to stirred soln. of Ir-complex over 1 h; filtered; evapd. (vac.); recrystd. from CH3CN/Et2O at room temp.; elem. anal.;
DOI:10.1021/om00051a018

Reference yield:

: 132959-02-5
IrOs(CO)5((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(CO)5(((C₆H₅)2P)2CH₂)2}BF₄

: 132939-86-7
IrOs(H)2(CO)3((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-) = {IrOs(H)2(CO)3(((C₆H₅)2P)2CH₂)2}BF₄

Guidance literature:: With H₂; In dichloromethane; stirred a soln. of Ir-complex under a stream of H2 for 36 h; evapd. (vac.); (31)P NMR; IR;
DOI:10.1021/om00051a018