(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

Base Information

Chemical Name:(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone
CAS No.:161443-50-1
Molecular Formula:C₃₂H₅₆O₃Si
Molecular Weight:516.88
Hs Code.:

Synonyms:(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

Chemical Property:

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Technology Process of (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

There total 1 articles about (3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125564-91-2
2-Trimethylsilanyl-oct-1-en-1-one

: 112763-97-0
(R)-3-phenylmethyloxy-tetradecanal

: (3S,4R)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

: (3S,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

: (3R,4R)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

: 161443-50-1
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

Guidance literature:: With ethylaluminum dichloride; In diethyl ether; toluene; at -40 - 0 ℃; Product distribution; other Lewis acid;
DOI:10.1055/s-1994-25684

Reference yield: 29.0%

: 161443-50-1
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

: 114264-05-0
(3S,4S)-4-((R)-2(benzyloxy)tridecyl)-3-hexyl-2-oxetanone

: 125638-37-1
(3R,4S)-3-hexyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -80 ℃; for 0.0833333h;
DOI:10.1055/s-1994-25684

Reference yield:

: 161443-50-1
(3R,4S)-3-hexyl-3-trimethylsilyl-4-<(R)-2'-(benzyloxy)tridecyl>-2-oxetanone

: 68711-40-0,104871-99-0,104872-00-6,104872-03-9,104872-05-1,104872-07-3,104872-19-7,104872-06-2
(3S,4S)-3-hexyl-4-[(R)-2-hydroxytridecyl]-2-oxetanone

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / 1M TBAF*3H₂O / tetrahydrofuran / 0.08 h / -80 °C

2: H₂ / 10percent Pd-C / tetrahydrofuran

With tetrabutyl ammonium fluoride; hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1055/s-1994-25684