4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

Base Information

Chemical Name:4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide
CAS No.:99275-66-8
Molecular Formula:C₁₈H₁₆N₂O₃
Molecular Weight:308.337
Hs Code.:

Synonyms:4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

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Chemical Property of 4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

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Technology Process of 4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

There total 3 articles about 4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 99275-60-2
2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-N-ethyl-N-phenyl-acetamide

: 99275-66-8
4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

Guidance literature:: With hydrogenchloride; sodium ethanolate; In ethanol; for 0.166667h; Heating;

Reference yield:

: 39086-61-8
2-chloro-N-ethylacetanilide

: 99275-66-8
4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / dimethylformamide / 4 h / 120 °C

2: 71 percent / 1.) sodium ethoxide; 2.) conc. HCl / ethanol / 0.17 h / Heating

With hydrogenchloride; sodium ethanolate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1074-82-4
potassium phtalimide

: 99275-66-8
4-Hydroxy-1-oxo-1,2-dihydro-isoquinoline-3-carboxylic acid ethyl-phenyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / dimethylformamide / 4 h / 120 °C

2: 71 percent / 1.) sodium ethoxide; 2.) conc. HCl / ethanol / 0.17 h / Heating

With hydrogenchloride; sodium ethanolate; In ethanol; N,N-dimethyl-formamide;