C₂₇H₂₉NO₃

Base Information

Chemical Name:C₂₇H₂₉NO₃
CAS No.:1335000-90-2
Molecular Formula:C₂₇H₂₉NO₃
Molecular Weight:415.532
Hs Code.:

C<sub>27</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:C₂₇H₂₉NO₃

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Chemical Property of C₂₇H₂₉NO₃

Chemical Property:

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Technology Process of C₂₇H₂₉NO₃

There total 10 articles about C₂₇H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335000-89-9
((2S,4S,5R)-1-benzyl-4-(benzyloxy)-5-(benzyloxymethyl)pyrrolidin-2-yl)methanol

: 1335000-90-2
C₂₇H₂₉NO₃

Guidance literature:: ((2S,4S,5R)-1-benzyl-4-(benzyloxy)-5-(benzyloxymethyl)pyrrolidin-2-yl)methanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 - -60 ℃; for 0.75h;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2011.06.018

Reference yield:

: C₂HF₃O₂*C₃₁H₄₁NO₇SSi

: 1335000-90-2
C₂₇H₂₉NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C

2.1: sodium tetrahydroborate / ethanol / 3 h / 20 °C

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 - -60 °C

5.2: 1 h / -78 - 20 °C

With sodium tetrahydroborate; oxalyl dichloride; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1016/j.tetasy.2011.06.018

Reference yield:

: 1335000-82-2
(S,E)-ethyl 5-(tert-butoxycarbonylamino)-6-(tert-butyldiphenylsilyloxy)hex-2-enoate

: 1335000-90-2
C₂₇H₂₉NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: osmium(VIII) oxide; methanesulfonamide; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / water; toluene; tert-butyl alcohol / 24 h / 0 °C

1.2: 0.75 h

2.1: triethylamine / dichloromethane / 72 h / 0 - 5 °C

3.1: dichloromethane / 2 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C

5.1: sodium tetrahydroborate / ethanol / 3 h / 20 °C

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 - -60 °C

8.2: 1 h / -78 - 20 °C

With sodium tetrahydroborate; osmium(VIII) oxide; oxalyl dichloride; methanesulfonamide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; dimethyl sulfoxide; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1.1: Sharpless dihydroxylation / 8.1: Swern oxidation / 8.2: Swern oxidation;
DOI:10.1016/j.tetasy.2011.06.018