C₃₃H₅₀N₂O₅Si

Base Information

Chemical Name:C₃₃H₅₀N₂O₅Si
CAS No.:1428850-18-3
Molecular Formula:C₃₃H₅₀N₂O₅Si
Molecular Weight:582.856
Hs Code.:

C<sub>33</sub>H<sub>50</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:C₃₃H₅₀N₂O₅Si

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Chemical Property of C₃₃H₅₀N₂O₅Si

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Technology Process of C₃₃H₅₀N₂O₅Si

There total 5 articles about C₃₃H₅₀N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1428850-12-7
C₂₂H₂₉IOSi

: 1428850-11-6
C₁₁H₂₂N₂O₄

: 1428850-18-3
C₃₃H₅₀N₂O₅Si

Guidance literature:: With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 70 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja401457h

Reference yield:

: 167102-72-9
(2R,3R) 2-<(tert-butoxycarbonyl)amino>-3-methyl-1,3-pentanediol

: 1428850-18-3
C₃₃H₅₀N₂O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; tetrabutyl-ammonium chloride; sodium hypochlorite / dichloromethane; water / 3 h / 0 °C / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / 1,2-dimethoxyethane / 0.17 h / -10 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

With 4-methyl-morpholine; sodium hypochlorite; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; caesium carbonate; potassium bromide; N,N`-dimethylethylenediamine; isobutyl chloroformate; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/ja401457h

Reference yield:

: 167102-74-1
(2S,3R)-2-tert-Butoxycarbonylamino-3-hydroxy-3-methyl-pentanoic acid

: 1428850-18-3
C₃₃H₅₀N₂O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / 1,2-dimethoxyethane / 0.17 h / -10 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 24 h / 70 °C / Inert atmosphere

With 4-methyl-morpholine; copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; isobutyl chloroformate; In 1,4-dioxane; 1,2-dimethoxyethane;
DOI:10.1021/ja401457h