sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

Base Information

Chemical Name:sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate
CAS No.:1103926-24-4
Molecular Formula:C₂₈H₂₈ClN₂O₆S*Na
Molecular Weight:579.049
Hs Code.:

Synonyms:sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

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Chemical Property of sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

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Technology Process of sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

There total 7 articles about sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1103928-79-5
tert-butyl 2-[(6-{[4-chloro-2-(methoxycarbonyl)phenyl]amino}-6-oxohexanoyl)amino]-4-phenylthiophene-3-carboxylate

: 1103926-24-4
sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 60 ℃; for 2h;
DOI:10.1248/cpb.59.215

Reference yield: 77.0%

: 1103926-24-4
sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

Guidance literature:

Reference yield:

: 944578-51-2
tert-butyl 2-amino-4-phenylthiophene-3-carboxylate

: 1103926-24-4
sodium 2-[(6-{[3-(tert-butoxycarbonyl)-4-phenylthiophen-2-yl]amino}-6-oxohexanoyl)amino]-5-chlorobenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 1,2-dimethoxyethane / 1 h / 0 - 20 °C

2: water; sodium hydroxide / tetrahydrofuran / 2.5 h / 60 °C

3: triethylamine / tetrahydrofuran / 1 h / 0 °C

4: tetrahydrofuran / 16 h / 0 - 20 °C

5: water; sodium hydroxide / tetrahydrofuran / 2 h / 60 °C

With water; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1248/cpb.59.215